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- Title
- EQUIBIAXIAL FLEXURAL STRENGTH TESTING OF ADVANCE CERAMICS.
- Creator
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Jordan, Ryan T, Orlovskaya, Nina, Kwok, Kawai; Ghosh, Ranajay, University of Central Florida
- Abstract / Description
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Ceramics are very important materials with many unique properties used in numerous industrial applications. Ceramics could be very hard and very strong in comparison to metals; however, they are very brittle, thus they are prone to instantaneous and catastrophic failure. Therefore, their reliability is compromised and it is very important to have advanced techniques that allow evaluating their mechanical behavior in many unusual stress states. One of such testing methods is biaxial strength...
Show moreCeramics are very important materials with many unique properties used in numerous industrial applications. Ceramics could be very hard and very strong in comparison to metals; however, they are very brittle, thus they are prone to instantaneous and catastrophic failure. Therefore, their reliability is compromised and it is very important to have advanced techniques that allow evaluating their mechanical behavior in many unusual stress states. One of such testing methods is biaxial strength method, that allows to measure properties not only unidirectional, but also in a biaxial way. The research work for this thesis will be built on design and development of ring-on-ring test jigs that will measure a biaxial strength of thin ceramic disks.
Show less - Date Issued
- 2018
- Identifier
- CFH2000386, ucf:45700
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFH2000386
- Title
- NONDESTRUCTIVE TESTING METHODS AIDED VIA NUMERICAL COMPUTATION MODELS FOR VARIOUS CRITICAL AEROSPACE AND POWER GENERATION SYSTEMS.
- Creator
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Warren, Peter, Ghosh, Ranajay, Raghavan, Seetha, Gou, Jihua, University of Central Florida
- Abstract / Description
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A current critical necessity for all industries which utilize various equipment that operates in hightemperature and extreme environments, is the ability to collect and analyze data via non destructivetesting (NDT) methods. Operational conditions and material health must be constantly monitoredif components are to be implemented precisely to increase the overall performance and efficiencyof the process. Currently in both aerospace and power generation systems there are many methodsthat are...
Show moreA current critical necessity for all industries which utilize various equipment that operates in hightemperature and extreme environments, is the ability to collect and analyze data via non destructivetesting (NDT) methods. Operational conditions and material health must be constantly monitoredif components are to be implemented precisely to increase the overall performance and efficiencyof the process. Currently in both aerospace and power generation systems there are many methodsthat are being employed to gather several necessary properties and parameters of a given system.This work will focus primarly on two of these NDT methods, with the ultimate goal of contributingto not only the method itself, but also the role of numerical computation to increase the resolutionof a given technique. Numerical computation can attribute knowledge onto the governing mechanicsof these NDT methods, many of which are currently being utilized in industry. An increase inthe accuracy of the data gathered from NDT methods will ultimately lead to an increase in operationalefficiency of a given system.The first method to be analyzed is a non destructive emmision technique widely referred to asaccoustic ultrasonic thermography. This work will investigate the mechanism of heat generationin acoustic thermography using a combination of numerical computational analysis and physicalexperimentation. Many of the challenges typical of this type of system are addressed in this work.The principal challenges among them are crack detection threshold, signature quality and the effectof defect interactions. Experiments and finite element based numerical simulations are employed,in order to evaluate the proposed method, as well as draw conclusions on the viability for futureextension and integration with other digital technologies for health monitoring. A method to determinethe magnitude of the different sources of heat generation during an acoustic excitation isalso achieved in this work. Defects formed through industrial operation as well as defects formedthrough artificial manufacturing methods were analyzed and compared.The second method is a photoluminescence piezospectroscopic (PLPS) for composite materials.The composite studied in this work has one host material which does not illuminate or have photoluminescenceproperties, the second material provides the luminescence properties, as well asadditional overall strength to the composite material. Understanding load transfer between the reinforcementsand matrix materials that constitute these composites hold the key to elucidating theirmechanical properties and consequent behavior in operation. Finite element simulations of loadingeffects on representative embedded alumina particles in a matrix were investigated and comparedwith experimental results. The alumina particles were doped with chromium in order to achieveluminscence capability, and therefore take advantage of the piezospectrscopic measurement technique.Mechanical loading effects on alumina nanoparticle composites can be captured with Photostimulated luminescent spectroscopy, where spectral shifts from the particles are monitored withload. The resulting piezospectroscopic (PS) coefficients are then used to calculate load transferbetween the matrix and particle. The results from the simulation and experiments are shown tobe in general agreement of increase in load transferred with increasing particle volume fractiondue to contact stresses that are dominant at these higher volume fractions. Results from this workpresent a combination of analytical and experimental insight into the effect of particle volume fractionon load transfer in ceramic composites that can serve to determine properties and eventuallyoptimize various parameters such as particle shape, size and dispersion that govern the design ofthese composites prior to manufacture and testing.
Show less - Date Issued
- 2018
- Identifier
- CFE0007262, ucf:52203
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0007262
- Title
- Design, Development, and Testing of a Miniature Fixture for Uniaxial Compression of Ceramics Coupled with In-Situ Raman Spectrometer.
- Creator
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Jordan, Ryan, Orlovskaya, Nina, Kwok, Kawai, Ghosh, Ranajay, University of Central Florida
- Abstract / Description
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This thesis is about the design, development and integration of an in-situ compression stage which interfaces through the Leica optical microscope coupled with a Renishaw InVia micro-Raman spectrometer. This combined compression stage and Raman system will enable structural characterization of ceramics and ceramic composites. The in-situ compression stage incorporates a 440C stainless steel structural components, 6061 aluminum frame, a NEMA 23 stepper motor. Two load screws that allow to...
Show moreThis thesis is about the design, development and integration of an in-situ compression stage which interfaces through the Leica optical microscope coupled with a Renishaw InVia micro-Raman spectrometer. This combined compression stage and Raman system will enable structural characterization of ceramics and ceramic composites. The in-situ compression stage incorporates a 440C stainless steel structural components, 6061 aluminum frame, a NEMA 23 stepper motor. Two load screws that allow to apply compressive loads up to 14,137 N, with negligible off axis loading, achieving target stresses of 500 MPa for samples of up to 6.00 mm in diameter. The system will be used in the future to study the structural changes in ceramics and ceramic composites, as well as to study thermal residual stress redistribution under applied compressive loads. A broad variety of Raman active ceramics, including the traditional structural ceramics 3mol%Y2O3-ZrO2, B4C, SiC, Si3N4, as well as exotic materials such as LaCoO3 and other perovskites will be studied using this system. Calibration of the systems load cell was performed in the configured state using MTS universal testing machines. To ensure residual stresses from mounting the load cell did not invalidate the original calibration, the in-situ compression stage was tested once attached to the Renishaw Raman spectrometer using LaCoO3 ceramic samples. The Raman shift of certain peaks in LaCoO3 was detected indicative of the effect of the applied compressive stress on the ceramics understudy.
Show less - Date Issued
- 2019
- Identifier
- CFE0007824, ucf:52809
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0007824
- Title
- INVESTIGATION OF PS-PVD AND EB-PVD THERMAL BARRIER COATINGS OVER LIFETIME USING SYNCHROTRON X-RAY DIFFRACTION.
- Creator
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Northam, Matthew, Raghavan, Seetha, Ghosh, Ranajay, Vaidyanathan, Raj, University of Central Florida
- Abstract / Description
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Extreme operating temperatures within the turbine section of jet engines require sophisticated methods of cooling and material protection. Thermal barrier coatings (TBCs) achieve this through a ceramic coating applied to a substrate material (nickel-based superalloy). Electron-beam physical vapor deposition (EB-PVD) is the industry standard coating used on jet engines. By tailoring the microstructure of an emerging deposition method, Plasma-spray physical vapor deposition (PS-PVD), similar...
Show moreExtreme operating temperatures within the turbine section of jet engines require sophisticated methods of cooling and material protection. Thermal barrier coatings (TBCs) achieve this through a ceramic coating applied to a substrate material (nickel-based superalloy). Electron-beam physical vapor deposition (EB-PVD) is the industry standard coating used on jet engines. By tailoring the microstructure of an emerging deposition method, Plasma-spray physical vapor deposition (PS-PVD), similar microstructures to that of EB-PVD coatings can be fabricated, allowing the benefits of strain tolerance to be obtained while improving coating deposition times. This work investigates the strain through depth of uncycled and cycled samples using these coating techniques with synchrotron X-ray diffraction (XRD). In the TGO, room temperature XRD measurements indicated samples of both deposition methods showed similar in-plane compressive stresses after 300 and 600 thermal cycles. In-situ XRD measurements indicated similar high-temperature in-plane and out-of-plane stress in the TGO and no spallation after 600 thermal cycles for both coatings. Tensile in-plane residual stresses were found in the YSZ uncycled PS-PVD samples, similar to APS coatings. PS-PVD samples showed in most cases, higher compressive residual in-plane stress at the YSZ/TGO interface. These results provide valuable insight for optimizing the PS-PVD processing parameters to obtain strain compliance similar to that of EB-PVD. Additionally, external cooling methods used for thermal management in jet engine turbines were investigated. In this work, an additively manufactured lattice structure providing transpiration cooling holes is designed and residual strains are measured within an AM transpiration cooling sample using XRD. Strains within the lattice structure were found to have greater variation than that of the AM solid wall. These results provide valuable insight into the viability of implementing an AM lattice structure in turbine blades for the use of transpiration cooling.
Show less - Date Issued
- 2019
- Identifier
- CFE0007844, ucf:52830
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0007844
- Title
- Investigation into the Feasibility of Adding Turbulators to Rocket Combustion Chamber Cooling Channels Using a Conjugate Heat Transfer Analysis.
- Creator
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Buchanan, Tyler, Kapat, Jayanta, Raghavan, Seetha, Ghosh, Ranajay, University of Central Florida
- Abstract / Description
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A conjugate heat transfer analysis will be carried out to simulate an 89 kN thrust chamber hydrogen cooling channel, to determine the feasibility of adding turbulators to the combustion chamber cooling channels at various parameters such as angle, pitch, and height of the turbulator. An existing regeneratively cooled chamber environment is simulated and used as a baseline case to be compared against. The new design includes using ribbed turbulators or delta wedges in the cooling channels to...
Show moreA conjugate heat transfer analysis will be carried out to simulate an 89 kN thrust chamber hydrogen cooling channel, to determine the feasibility of adding turbulators to the combustion chamber cooling channels at various parameters such as angle, pitch, and height of the turbulator. An existing regeneratively cooled chamber environment is simulated and used as a baseline case to be compared against. The new design includes using ribbed turbulators or delta wedges in the cooling channels to increase the heat transfer on the channel hot wall (wall adjacent to the hot gas wall) and on the two channel sidewalls. With a higher heat transfer coefficient, the sidewalls behave like fins for heat transfer and participate more in the overall heat transfer process in the channel. Efficient rib and wedge geometries are chosen based on previous investigations. A conjugate heat transfer analysis is performed using a straight duct with the rib and wedge geometries included, with boundary conditions similar to those found in the combustion chamber, to provide thermal hydraulic performance data at numerous turbulator configurations. The baseline channel's maximum hot wall temperature is the target maximum hot wall temperature that is desired to be reduced. The goal is to reduce the hot gas side wall temperature at a minimal cost in pressure drop.
Show less - Date Issued
- 2018
- Identifier
- CFE0007160, ucf:52320
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0007160
- Title
- Characterization of Turbulent Flame-Vortex Dynamics for Bluff Body Stabilized Flames.
- Creator
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Rising, Cal, Ahmed, Kareem, Ghosh, Ranajay, Bhattacharya, Samik, University of Central Florida
- Abstract / Description
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Modern propulsion systems primarily operate under highly turbulent conditions in order to promote greater efficiency through an increase in mixing. The focus of this thesis is to identify the turbulent flame-vortex interaction to provide insights into the turbulent combustion process. This work is accomplished through the use of turbulent ramjet-style combustor which is stabilized through use of a bluff-body. The facility is equipped with a custom turbulence generator to modulate the incoming...
Show moreModern propulsion systems primarily operate under highly turbulent conditions in order to promote greater efficiency through an increase in mixing. The focus of this thesis is to identify the turbulent flame-vortex interaction to provide insights into the turbulent combustion process. This work is accomplished through the use of turbulent ramjet-style combustor which is stabilized through use of a bluff-body. The facility is equipped with a custom turbulence generator to modulate the incoming turbulence levels to allow flames across various regimes to be analyzed. High-speed particle image velocimetry (PIV) and CH* chemiluminescence diagnostics are implemented to resolve the flow field and flame position. The flame-vortex interaction can be described by the vorticity transport which has four terms; vortex stretching, baroclinic torque, dilatation, and viscous diffusion. The vorticity mechanisms are calculated through the implementation of a Lagrangian tracking scheme, which allows for the individual mechanisms to be decomposed along the path of individual tracks. The mechanisms are compared across different turbulence levels to determine the effects of turbulence on the vorticity mechanisms. The mechanisms are calculated along the flame front as well to determine the individual effects of the vorticity mechanisms on the evolving structure of the turbulent premixed flame. The flame front curvature is also compared across the various turbulence conditions. The results confirm that as the flame-front experiences increased turbulence levels the combustion induced mechanisms of baroclinic torque and dilation decrease, while vortex stretching increases. This is a result of the turbulent energy exchange becoming the controlling factor within the flow-field. In addition, increased flame curvature is experience by the flame front due to increased local baroclinicity and turbulent energy exchange.
Show less - Date Issued
- 2019
- Identifier
- CFE0007714, ucf:52451
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0007714
- Title
- Analysis of residual stress and damage mechanisms of thermal barrier coatings deposited via PS-PVD and EB-PVD.
- Creator
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Rossmann, Linda, Raghavan, Seetha, Sohn, Yongho, Vaidyanathan, Raj, Ghosh, Ranajay, University of Central Florida
- Abstract / Description
-
Thermal barrier coatings (TBCs) are critical to gas turbine engines, as they protect the components in the hot section from the extreme temperatures of operation. The current industry standard method of applying TBCs for turbine blades in jet engines is electron-beam physical vapor deposition (EB-PVD), which results in a columnar structure that is valued for its high degree of strain tolerance. An emerging deposition method is plasma-spray physical vapor deposition (PS-PVD), capable of...
Show moreThermal barrier coatings (TBCs) are critical to gas turbine engines, as they protect the components in the hot section from the extreme temperatures of operation. The current industry standard method of applying TBCs for turbine blades in jet engines is electron-beam physical vapor deposition (EB-PVD), which results in a columnar structure that is valued for its high degree of strain tolerance. An emerging deposition method is plasma-spray physical vapor deposition (PS-PVD), capable of producing a variety of customizable microstructures as well as non-line-of-sight deposition, which allows more complex geometries to be coated, or even multiple parts at once. The pseudo-columnar microstructure that can be produced with PS-PVD is a possible alternative to EB-PVD. However, before PS-PVD can be used to its full potential, its mechanical properties and behavior must be understood. This work contributes to this understanding by characterizing PS-PVD TBCs that have been thermally cycled to simulate multiple lifetimes (0, 300, and 600 thermal cycles). Residual stress in the thermally grown oxide (TGO) layer is characterized by photoluminescence piezospectroscopy as TGO residual stress is correlated with the lifetime of the coating. Residual stress in the top coat is characterized by Raman spectroscopy, because this stress drives cracking in the top coat that can lead to failure. Scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS) are performed to observe microstructural and phase evolution to provide context and possible explanations for the stress results. In addition, EB-PVD samples of the same thermal cycling history are characterized in the same way so that PS-PVD can be benchmarked against the industry standard. The compressive residual stress in the TGO in both coatings was relieved with thermal cycling due to the TGO lengthening as well as microcracking. The PS-PVD samples had slightly lower TGO stress than the EB-PVD, which is attributed to the greater extent of cracking within the TGO, whereas cracking in the EB-PVD samples was at the TGO/topcoat interface. The PS-PVD cycled samples had significant cracking within the topcoat near the TGO due to both greater porosity than EB-PVD samples and regions of unmelted particles that provide little resistance to cracking. The greater convolution of the TGO in the PS-PVD samples results in greater out-of-plane tensile stresses that cause crack initiation, as well as diverts cracks away from the difficult-to-follow interface. The TGO stress results agree with existing literature and extend the thermal cycling beyond what has previously been reported for PS-PVD coatings, revealing a trend of stress relief and stress values similar to that of EB-PVD coatings in this study and in the literature. Residual stress in the topcoat for both coating types became increasingly compressive with thermal cycling, indicating loss of strain tolerance by sintering. The trend of the YSZ stress for both coating types to become more compressive with cycling and with depth agrees with the literature, and the thermal cycling is longer than has been previously reported for PS-PVD. The two coating types had quite different microstructures and crack modes as well as different as-deposited residual stresses, but after thermal cycling had similar stresses in both the TGO and top coat. No samples experienced spallation. These results indicate that, while PS-PVD coatings have different properties and behavior from EB-PVD coatings, they had comparable levels of damage to EB-PVD coatings of the same lifetime and are a viable alternative to EB-PVD. Further tuning of the processing parameters may result in PS-PVD coatings with even more similar behavior to EB-PVD coatings.
Show less - Date Issued
- 2019
- Identifier
- CFE0007717, ucf:52429
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0007717
- Title
- Shape Recovery Behavior of Carbon Nanopaper Shape Memory Polymer Composite.
- Creator
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Ozdemir, Veli Bugra, Kwok, Kawai, Gou, Jihua, Ghosh, Ranajay, University of Central Florida
- Abstract / Description
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This thesis presents analytical, experimental and modeling studies of the shape recovery behavior of electrically activated Carbon Nanopaper (CNP) Shape Memory Polymer (SMP)composite. The composite structure studied consists of a CNP layer sandwiched by two SMP layers where the CNP layer acts as a ?exible electrical heater when a voltage difference is applied. The behavior of CNP/SMP composite presents a coupled electrical - thermal - structural problem. The governing equations for the...
Show moreThis thesis presents analytical, experimental and modeling studies of the shape recovery behavior of electrically activated Carbon Nanopaper (CNP) Shape Memory Polymer (SMP)composite. The composite structure studied consists of a CNP layer sandwiched by two SMP layers where the CNP layer acts as a ?exible electrical heater when a voltage difference is applied. The behavior of CNP/SMP composite presents a coupled electrical - thermal - structural problem. The governing equations for the multiphysics behavior are derived. Derived parameters as a result of multiphysics analysis and effects of these parameters on the shape recovery behavior are investigated. The mechanical properties of the carbon nanopaper and viscoelastic properties of the shape memory polymer are characterized. A nonlinear, fully coupled electrical -thermal-structural ?nite element model is developed, and shape recovery experiments are carried out to validate multiphysics analysis and ?nite element model of the shape recovery of the CNP/SMP composite. Finite element model captures the general behavior of shape recovery, but overpredicts shape ?xity and shape recovery rate.
Show less - Date Issued
- 2019
- Identifier
- CFE0007700, ucf:52417
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0007700
- Title
- Development and Implementation of a Streamlined Process for the Creation and Mechanization of Negative Poisson's Ratio Meso-Scale Patterns.
- Creator
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Shuler, Matthew, Gordon, Ali, Kauffman, Jeffrey L., Ghosh, Ranajay, University of Central Florida
- Abstract / Description
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This thesis focuses on the development a streamlined process used to create novel meso-scale pattern used to induce negative Poisson's ratio (NPR) behavior at the bulk scale. This process includes, the development, optimization, and implementation of a candidate pattern. Currently, the majority of NPR structures are too porous to be utilized in conventional applications. For others, manufacturing methods have yet to realize the meso-scale pattern. Consequently, new NPR meta-materials must be...
Show moreThis thesis focuses on the development a streamlined process used to create novel meso-scale pattern used to induce negative Poisson's ratio (NPR) behavior at the bulk scale. This process includes, the development, optimization, and implementation of a candidate pattern. Currently, the majority of NPR structures are too porous to be utilized in conventional applications. For others, manufacturing methods have yet to realize the meso-scale pattern. Consequently, new NPR meta-materials must be developed in order to confer transformative thermomechanical responses to structures where transverse expansion is more desirable than contraction. For example, materials at high temperature. Additionally, patterns that take into account manufacturing limitations, while maintaining the properties characteristically attached to negative Poisson's Ratio materials, are ideal in order to utilize the potential of NPR structures. A novel NPR pattern is developed, numerically analyzed, and optimized via design of experiments. The parameters of the meso-structure are varied, and the bulk response is studied using finite element analysis (FEA). The candidate material for the study is Medium-Density Fiberboard (MDF). This material is relevant to a variety of applications where multiaxial stresses, particularly compressive, lead to mechanical fatigue. Samples are fabricated through a laser cutting process, and a comparison is drawn through the use of experimental means, including traditional tensile loading tests and digital image correlation (DIC). Various attributes of the elasto-plasticity responses of the bulk structure are used as objectives to guide the optimization process.
Show less - Date Issued
- 2017
- Identifier
- CFE0006795, ucf:51830
- Format
- Document (PDF)
- PURL
- http://purl.flvc.org/ucf/fd/CFE0006795