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A METHODOLOGY FOR INSTRUMENTED INDENTATION STUDIES OF DEFORMATION IN BULK METALLIC GLASSES
Title
A METHODOLOGY FOR INSTRUMENTED INDENTATION STUDIES OF DEFORMATION IN BULK METALLIC GLASSES.
Creator
Sridharan, Subhaashree, Vaidyanathan, Raj, University of Central Florida
Abstract / Description
Bulk Metallic Glasses (BMGs), also known as amorphous metals, are of considerable scientific and commercial interest due to their random or chaotic structure. Given their potential use as engineering materials, there is a concomitant need to establish their mechanical properties. However, BMGs are not conveniently available in sufficient volumes (especially experimental and combinatorial compositions), making property determination via conventional tensile or compression testing problematic....
Show moreBulk Metallic Glasses (BMGs), also known as amorphous metals, are of considerable scientific and commercial interest due to their random or chaotic structure. Given their potential use as engineering materials, there is a concomitant need to establish their mechanical properties. However, BMGs are not conveniently available in sufficient volumes (especially experimental and combinatorial compositions), making property determination via conventional tensile or compression testing problematic. Instrumented indentation is ideally suited for this purpose because the testing requires only small sampling volumes and can probe multiaxial deformation characteristics at various length scales. In this technique, conducted generally on a sub-micron regime, the depth of penetration of an indenter, usually a diamond, is measured as a function of the applied load and expressed graphically as load (P) - displacement (h) curves from which a host of mechanical properties can be extracted and studied. In this work, a methodology for using instrumented indentation at nano- and micro- scales to determine the mechanical response of BMGs was developed and implemented. The implementation primarily focused on deformation in the elastic regime but included preliminary results related to the onset of inelastic deformation. The methodology developed included calibration techniques, formulations to extract the machine compliances, verifications using standards and verification for uniqueness of instrument deformation under a spherical indenter. The methodology was different for the two platforms used based on the load-depth response characteristics of the instrument. In the case of the Micro Test platform, the load-depth response of the instrument was linear. In the case of the Nano Test platform, the instrument load-depth response followed a 3/2 power law, representative of Hertzian behavior. The load-depth response of the instrument was determined by subtracting the theoretical response from the corresponding raw load-depth response obtained by elastically indenting a standard steel specimen of known modulus. The true response of the sample was then obtained by subtracting the instrument's response from the corresponding uncorrected load-depth response (raw data). An analytical model to describe the load-train compliance was developed. The methodology was verified using quartz and tungsten standards. Indentation experiments were conducted on Zr41.25Ti13.75Cu12.5Ni10Be22.5 (Vitreloy 1), Cu60Hf25Ti15, Cu60Zr30Ti10 and Fe60Co7Zr10Mo5W2B16 bulk metallic glasses using spherical indenters with diameters 2.8 mm and 100 m. The spherical geometry results in a simpler stress distribution under the indenter (when compared to a sharp geometry) and furthermore by recourse to spherical indenters the onset of plastic deformation was delayed. In the case of the Zr-based BMG, the experiments showed that the elastic response did not depend on the diameter of the indenter used indicative of the absence of residual stresses in the sample. Large scale plastic deformation was observed when the sample was indented using a smaller diameter indenter. Log scale analysis (i.e., examining the results on a log load vs. log depth response to check for deviation from Hertzian behavior) showed a deviation from a 3/2 fit indicating a deviation from elastic behavior. The onset implied a yield strength value of ~ 4 GPa, higher than the value reported in the literature (~ 2 GPa). Hence, it is believed that the first signs of plastic deformation occurred at lower loads than the predicted loads from the log scale analysis procedure and is expected to occur as discrete bursts. Discrete plastic events or "pop-ins" were observed in the load-depth indentation responses under quasistatic loading conditions, which were believed to be associated with shear band activity. An attempt was made to formulate a mathematical model based on three yield criteria (Drucker-Prager, Mohr-Coulomb and von Mises). Based on the von Mises predictions and comparable experiments on a quartz standard, it was established that the pop-ins observed were real and not an instrument artifact. Multiple load cycles following partial unload experiments showed that the pop-ins affected the subsequent indentation response. The moduli and the yield strength values obtained for the Cu-based BMGs were comparable to the values reported in the literature. There was significant scatter in the indentation data from the Fe-based BMG. Porosity and lack of 100 % compaction were believed to be the reasons for scatter in the data. The financial support of NSF through grant DMR 0314212 is gratefully acknowledged.
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Date Issued
2006
Identifier
CFE0001442, ucf:47047
Format
Document (PDF)
PURL
http://purl.flvc.org/ucf/fd/CFE0001442
MECHANICAL CHARACTERIZATION AND NUMERICAL SIMULATION OF A LIGHT-WEIGHT ALUMINUM A359 METAL-MATRIX COMPOSITE
Title
MECHANICAL CHARACTERIZATION AND NUMERICAL SIMULATION OF A LIGHT-WEIGHT ALUMINUM A359 METAL-MATRIX COMPOSITE.
Creator
DeMarco, James, Gordon, Ali, University of Central Florida
Abstract / Description
Aluminum metal-matrix composites (MMCs) are well positioned to replace steel in numerous manufactured structural components, due to their high strength-to-weight and stiffness ratios. For example, research is currently being conducted in the use of such materials in the construction of tank entry doors, which are currently made of steel and are dangerously heavy for military personnel to lift and close. However, the manufacture of aluminum MMCs is inefficient in many cases due to the loss of...
Show moreAluminum metal-matrix composites (MMCs) are well positioned to replace steel in numerous manufactured structural components, due to their high strength-to-weight and stiffness ratios. For example, research is currently being conducted in the use of such materials in the construction of tank entry doors, which are currently made of steel and are dangerously heavy for military personnel to lift and close. However, the manufacture of aluminum MMCs is inefficient in many cases due to the loss of material through edge cracking during the hot rolling process which is applied to reduce thick billets of as-cast material to usable sheets. In the current work, mechanical characterization and numerical modeling of as-cast aluminum A359-SiCp-30% is employed to determine the properties of the composite and identify their dependence on strain rate and temperature conditions. Tensile and torsion tests were performed at a variety of strain rates and temperatures. Data obtained from tensile tests were used to calibrate the parameters of a material model for the composite. The material model was implemented in the ANSYS finite element software suite, and simulations were performed to test the ability of the model to capture the mechanical response of the composite under simulated tension and torsion tests. A temperature- and strain rate-dependent damage model extended the constitutive model to capture the dependence of material failure on testing or service conditions. Trends in the mechanical response were identified through analysis of the dependence of experimentally-obtained material properties on temperature and strain rate. The numerical model was found to adequately capture strain rate and temperature dependence of the stress-strain curves in most cases. Ductility modeling allowed prediction of stress and strain conditions which would lead to rupture, as well as identification of areas of a solid model which are most likely to fail under a given set of environmental and load conditions.
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Date Issued
2011
Identifier
CFE0004007, ucf:49177
Format
Document (PDF)
PURL
http://purl.flvc.org/ucf/fd/CFE0004007
Design, Development, and Testing of a Miniature Fixture for Uniaxial Compression of Ceramics Coupled with In-Situ Raman Spectrometer
Title
Design, Development, and Testing of a Miniature Fixture for Uniaxial Compression of Ceramics Coupled with In-Situ Raman Spectrometer.
Creator
Jordan, Ryan, Orlovskaya, Nina, Kwok, Kawai, Ghosh, Ranajay, University of Central Florida
Abstract / Description
This thesis is about the design, development and integration of an in-situ compression stage which interfaces through the Leica optical microscope coupled with a Renishaw InVia micro-Raman spectrometer. This combined compression stage and Raman system will enable structural characterization of ceramics and ceramic composites. The in-situ compression stage incorporates a 440C stainless steel structural components, 6061 aluminum frame, a NEMA 23 stepper motor. Two load screws that allow to...
Show moreThis thesis is about the design, development and integration of an in-situ compression stage which interfaces through the Leica optical microscope coupled with a Renishaw InVia micro-Raman spectrometer. This combined compression stage and Raman system will enable structural characterization of ceramics and ceramic composites. The in-situ compression stage incorporates a 440C stainless steel structural components, 6061 aluminum frame, a NEMA 23 stepper motor. Two load screws that allow to apply compressive loads up to 14,137 N, with negligible off axis loading, achieving target stresses of 500 MPa for samples of up to 6.00 mm in diameter. The system will be used in the future to study the structural changes in ceramics and ceramic composites, as well as to study thermal residual stress redistribution under applied compressive loads. A broad variety of Raman active ceramics, including the traditional structural ceramics 3mol%Y2O3-ZrO2, B4C, SiC, Si3N4, as well as exotic materials such as LaCoO3 and other perovskites will be studied using this system. Calibration of the systems load cell was performed in the configured state using MTS universal testing machines. To ensure residual stresses from mounting the load cell did not invalidate the original calibration, the in-situ compression stage was tested once attached to the Renishaw Raman spectrometer using LaCoO3 ceramic samples. The Raman shift of certain peaks in LaCoO3 was detected indicative of the effect of the applied compressive stress on the ceramics understudy.
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Date Issued
2019
Identifier
CFE0007824, ucf:52809
Format
Document (PDF)
PURL
http://purl.flvc.org/ucf/fd/CFE0007824